Giơi thiệu sản phẩm

TRIFLUOROMETHANESULFONYL CHLORIDE;TRIFLUOROMETHANESULPHONYL CHLORIDE;TRIFLYL CHLORIDE;Methanesulfonyl chloride, trifluoro-;PFC-MSC;Trifluoromathanesulfonyl chloride;Trifluoromethanesulphonylchloride,99%;trifluoromethylsulfonyl chloride
421-83-0
CClF3O2S
168.52
207-009-0
421-83-0.mol
Trifluoromethanesulfonyl chloride Structure
 
-26 degree
29-32 degree (lit.)
1.583 g/mL at 25 degree (lit.)
10.36 psi ( 20 degree )
n20/D 1.334(lit.)
32 degree
2-8 degree
1.583
1812016
GRGCWBWNLSTIEN-UHFFFAOYSA-N
421-83-0(CAS DataBase Reference)
 
C
14-34
26-36/37/39-45
UN 3265 8/PG 2
3
F 10-21
8
29049090
 
 
Ru(II) complex-catalyzed trifluoromethylating agent for aromatics and alkenes.



Add 150g (1mol) of trifluoromethanesulfonic acid to the reactor equipped with thermometer, distillation device and mechanical stirrer, slowly add 435mL (6mol) of thionyl chloride under ice bath, and then add the catalyst N,N-dimethyl Formamide 7.36 (0.1 mol), slowly raise the temperature to room temperature, stir for half an hour, continue to heat up to 40 degree , continue to stir, react for 12 hours, and then drop to room temperature after the reaction is complete.Subsequently, vacuum distillation was carried out at 110 degree C. and -0.1 to -0.08 MPa, and at the same time, the temperature was slowly raised to 50 degree C. to obtain 147 g of trifluoromethanesulfonyl chloride, with a yield of 87.5%. TRIFLUOROMETHANESULFONYL CHLORIDE
 
N-Phenyl-bis(trifluoromethanesulfonimide)-->2,2,3,3,3-PENTAFLUOROPROPYL TRIFLUOROMETHANESULFONATE-->1-NAPHTHYL TRIFLATE-->N-Hydroxynaphthalimide triflate-->1-(TRIFLUOROMETHANESULFONYL)IMIDAZOLE-->1-ADAMANTYL ISOTHIOCYANATE-->4-NITROPHENYL TRIFLUOROMETHANESULFONATE-->Methyl trichloroacetate-->

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